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Reaction of trans-Stilbene with Hydrobromic Acid and Hydrogen Peroxide Chemistry 251 Fall 2012 Background This semester you will learn many electrophilic addition reactions to alkenes, including hydrohalogenation, hydration, halohydrin, and halogenation as well as the radical addition of HBr to an alkene. In this lab, your task is to figure out ...

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SOURCE: All reaction diagrams were pieced together from the UChicago Organic Chemistry Lab Manual by Valerie Keller. Results: Yield of Multistep Synthesis: Synthesis of meso-dibromostilbene : 1.0 g trans -stilbene (5.55E-3 mol) used with 2.0 g pyridinium tribromide (6.25E-3 mol); thus, trans- stilbene is expected to be limiting reagent.

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Page 152 Metalated heterocycles in organic synthesis: recent applications Rafael Chinchilla,* Carmen Nájera,* and Miguel Yus* Departamento de QuĂ­mica Orgánica and Instituto de SĂ­ntesis Orgánica (ISO), Universidad de Alicante, Apartado 99, 03080 Alicante, Spain E-mails: [email protected], [email protected], [email protected] Dedicated to Professor Alain Krief on occasion of his 65th birthday Contents 1.

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[Organic Chemistry -Reaction and Synthesis- Metallo-organic Chemistry] (Bldg.10 1011) Room F2 [Organic Chemistry -Reaction and Synthesis- Metallo-organic Chemistry] (Bldg.10 1012) Room F3 [Organic Chemistry -Reaction and Synthesis- Metallo-organic Chemistry] (Bldg.10 1013) Room F4 Jul 19, 2011 · What You Actually Do This Week in Lab, and Sample Calculations. This week you’re going to react cyclopentadiene with maleic anhydride to form the Diels-Alder adduct: You will dissolve ~4g of maleic anhydride (be sure to measure the exact amount) in ~15 mL of ethyl acetate (EtOAc) in a 125mL Erlenmeyer flask.

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Since this lab will be over a 3 week period, this will serve as three labs, and the entire lab will be worth 150 points. The points will be divided up as usual, but just take those amounts and multiply by 3. This means that your lab report will be worth 60 points.

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Procedure - Preparation of Diphenylacetylene from Stilbene Dibromide Place approximately 3 g of potassium hydroxide into a 100 mL round-bottom flask and add 30 mL of ethylene glycol and a magnetic stir bar. Check to be sure the lab jack holding your hot plate is raised a few inches.

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